Analyse using x-ray fluorescence


Peat extracted from Wessenden Moor in West Yorkshire in November 2002. Samples of 2cm diameter were analysed taken from a 50cm deep core. Different depths of the peat core were analysed using X-Ray Fluorescence (XRF) analysis to measure the concentration of Iron, Lead, Bromine and Calcium. The results obtained after performing XRF analysis are shown in table.

Table:Results of XRF analysis of a peat core extracted from Wessenden Moor, November 2002

Elements
Fe Pb Br Ca
midpoint cm cm depth (mg kg-1) (mg kg-1) (mg kg-1) (mg kg-1)
1 00-02 18630 451.7 95.2 1828
5 04-06 25350 816.0 72.0 1465
11 10-12 5244 299.0 65.3 1631
15 14-16 5258 116.3 58.0 1597
21 20-22 4692 29.8 68.3 1954
25 24-26 3324 22.5 57.1 1986
31 30-32 2039 19.2 69.5 1467
41 40-42 2707 21.8 61.5 965.5
49 48-50 2163 25.0 77.4 1471

The peat core was obtained from Wessenden Moor, 4 meters west of Holmfirth, 500 meters north of A635 Holmfirth Road.

Samples 2cm x 2cm from the core which was 50 cm long from the surface (zero cm) were taken. (Full depth of the peat is about 225cm)

The peat was dried at 80oC for 3 days, ground and 4g analysed quantitatively in the XRF spectrometer against internal standards.

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